42417-39-0, 3-Aminodihydrofuran-2(3H)-one hydrochloride is a Tetrahydrofurans compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Synthesis of Butoxy-SHL (1) To a solution of 3,4-dibutoxy-cyclobut-3-ene-1,2-dione (0.120 g, 0.53 mmol) in DMF at rt was added alpha-Amino-gamma-butyrolactone-hydrochloride (0.070 g, 0.38 mmol) and triethylamine (1.5 equiv.) and the mixture refluxed overnight. The completion of the reaction was monitored by TLC for the disappearance of starting material. The reaction was quenched with water and extracted with EtOAc (3*100 mL). The organic layers were collected, washed with brine (2*25 mL), dried over Na2SO4 and concentrated in vacuo. Flash column chromatography (SiO2, 100% EtOAc) yielded compound 1 as a brown solid.
42417-39-0, 42417-39-0 3-Aminodihydrofuran-2(3H)-one hydrochloride 445963, aTetrahydrofurans compound, is more and more widely used in various fields.
Reference£º
Patent; SYRACUSE UNIVERSITY; Luk, Yan-Yeung; Narasimhan, Sri Kamesh; Falcone, Eric; US2014/39195; (2014); A1;,
Tetrahydrofuran – Wikipedia
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