Spanik, I. published the artcileA comparative study of various sample preparation procedures for characterization of organic compounds in brandy, SDS of cas: 19444-84-9, the publication is Uchenye Zapiski Kazanskogo Universiteta, Seriya Estestvennye Nauki (2014), 156(4), 8-28, database is CAplus.
This paper describes the composition of volatile compounds in 19 different wine distillates was studied by gas chromatog. (GC) coupled with flame ionization (FID) or mass-spectrometric (MS) detector. The studied samples were divided into two groups depending on the way of their production and geog. region. The effect of various sample treatment procedures on final composition of volatiles was investigated in details. The effectiveness of direct injection, headspace, solid phase extraction (SPE), solid phase microextraction (SPME) and liquid-liquid extraction (LLE) was compared. Moreover, the effect of exptl. conditions of preconcentration methods such as type of sorbent, temperature, time or solvent removal procedure was studied in details. The repeatability of particular sample preparation procedure was evaluated by comparison of peak areas for randomly selected compounds obtained from 4 parallel measurements. It was shown that the most suitable sample treatment procedure in terms of repeatability is SPE followed by direct injection and headspace. LLE and SPME provide higher variability of peak areas, thus utilization of internal standard for quantification is recommended. On the contrary, the most suitable sample treatment procedure in terms of the number of different type of compounds is liquid-liquid extraction into CH2Cl2. By this method, more than 240 compounds have been extracted from wine distillates produced by classical technol. Furthermore, SPME has shown different selectivity which allows one to determine compounds that could not be extracted by other studied sample preparation methods.
Uchenye Zapiski Kazanskogo Universiteta, Seriya Estestvennye Nauki published new progress about 19444-84-9. 19444-84-9 belongs to tetrahydrofurans, auxiliary class Tetrahydrofuran,Ester,Alcohol, name is 3-Hydroxydihydrofuran-2(3H)-one, and the molecular formula is C30H24BrCuN2P, SDS of cas: 19444-84-9.
Referemce:
https://en.wikipedia.org/wiki/Tetrahydrofuran,
Tetrahydrofuran | (CH2)3CH2O – PubChem