Discovery of Ethyl 2-oxotetrahydrofuran-3-carboxylate

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Silica gel was found to mediate decarboxylation of tetracarbonyl compounds with a free carboxylic group prepared from beta-dicarbonyl compounds and malonyl peroxides. Under solvent-free heterogeneous conditions silica gel effectively acts as a mediator of C?O coupling with further decarboxylation at 120 C.

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Reference：
Tetrahydrofuran – Wikipedia,
Tetrahydrofuran | (CH2)3CH2O – PubChem